Improved Process for Preparation of tert-Butanesulfinyl Ketimines of Hindered Ketones under Nitrogen Flow

DOI: 10.1021/acs.oprd.6b00188

Source and publish data:

Organic Process Research and Development p. 1383 - 1387 (2016)

Update date:2022-07-30

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Authors:

Tabet, Samuel

Rodeville, Nicolas

Boiteau, Jean-Guy

Cardinaud, Isabelle

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Article abstract of DOI:10.1021/acs.oprd.6b00188

An improved process for tert-butanesulfinyl ketimines formation using titanium(IV) alkoxides is described. This new protocol gives better results especially for sterically hindered ketones compared to classical conditions where titanium(IV) isopropoxide i

Full text of DOI:10.1021/acs.oprd.6b00188

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