Main Group Metal Chemistry p. 87 - 91 (2017)
Update date:2022-09-26
Topics:
Xie, Xiaoqiang
Qi, Weipeng
Sun, Xinzhe
Zhang, Xingxian
The aldol addition of acyldiazomethane with aromatic aldehydes, vinyl aldehyde and aliphatic aldehydes was carried out efficiently in the presence of MgI2 etherate and iPr2EtN (DIPEA) using untreated reagent-grade CH2Cl2 under atmospheric conditions in good to excellent yields. Iodide counterion and a non-coordinating reaction media (i.e. CH2Cl2) are among the critical factors for the unique reactivity of this reaction system.
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