Tetrahedron Letters p. 4425 - 4428 (1983)
Update date:2022-07-29
Topics:
Elphimoff-Felkin, Irene
Sarda, Pierre
Clemmensen reduction (zinc and hydrogen chloride in dry diethyl ether) of 1-methoxy- and 1,5-dimethoxy-cyclohexa-1,4-diene affords the cyclopropyl ethers, 1-methoxy- and 1,5-dimethoxy-bicyclo<3.1.0>hexane; in the presence of acetic anhydride, reduction of 6-acetyl-1-methoxy-6-methyl-cyclohexa-1,4-diene leads regiospecifically to 7-acetoxy-1-methoxy-6,7-dimethyl-bicyclo<4.1.0>hept-4-ene.
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