Stereoselective Synthesis of Squalamine Dessulfate

DOI: 10.1016/00404-0399(50)10116-

Source and publish data:

Tetrahedron Letters p. 5139 - 5142 (1995)

Update date:2022-08-02

Topics:

Authors:

Moriarty, Robert M.

Enache, Livia A.

Kinney, William A.

Allen, Craig S.

Canary, James W.

et al. et al.

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Article abstract of DOI:10.1016/00404-0399(50)10116-

Squalamine dessulfate (24R) and the unnatural product squalamine dessulfate (24S) have been synthesized from stigmasterol.The key step is establishing the C24 stereochemistry is attachment of the sidechain at C22 using either (2R)- or (2S)-1,2-epoxy-3-met

Full text of DOI:10.1016/00404-0399(50)10116-

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Product name:(24R)-6β-methoxy-22-phenylsulfonyl-24-hydroxy-3α,5α-cyclocholestane

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