Journal of Organic Chemistry p. 2242 - 2249 (2020)
Update date:2022-08-11
Topics:
Han, Xingyou
Li, Feng
Liu, Peng
Wang, Rongzhou
Xu, Jing
An anionic iridium complex [Cp*Ir(2,2′-bpyO)(OH)][Na] was found to be a general and highly efficient catalyst for transfer hydrogenation of ketones and imines with methanol under base-free conditions. Readily reducible or labile substituents, such as nitro, cyano, and ester groups, were tolerated under present reaction conditions. Notably, this study exhibits the unique potential of anionic metal-ligand bifunctional iridium catalysts for transfer hydrogenation with methanol as a hydrogen source.
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