A new and easy synthesis of silylated furanoid glycals in one step from nucleotides

DOI: 10.1055/s-1994-25633

Source and publish data:

Synthesis p. 1037 - 1038 (1994)

Update date:2022-08-11

Topics:

Authors:

Larsen Larsen

Jorensen

Sofan Sofan

Pedersen

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Article abstract of DOI:10.1055/s-1994-25633

Silylated furanoid glycals are synthesized in high yields by elimination of the nucleobase in thymidine (1a) and 5'-O-(tert-butyldiphenylsilyl)thymidine (1b) on treatment with 1,1,1,3,3,3-hexamethyldisilazane (HMDS) in the presence of ammonium sulfate at

Full text of DOI:10.1055/s-1994-25633

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