Journal of the American Chemical Society p. 6311 - 6314 (1980)
Update date:2022-08-10
Topics:
Scott, Lawrence T.
Minton, Mark A.
Kirms, Mark A.
A short new azulene synthesis requiring no dehydrogenation step, has been developed (Scheme 1).Intramolecular carbene addition creates the bicyclic ring system of azulene with a high degree of unsaturation and versatile functionality in a single step from a simple benzene derivative.The synthesis is particularly amenable to preparation of specific 13C- and 2H-labeled azulenes.
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