Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 1528 - 1530 (1990)
Update date:2022-08-17
Topics:
Polivin, Yu. N.
Vinokurov, V. A.
Makarshin, S. V.
Karakhanov, R. A.
Silin, M. A.
Ageev, E. A.
Chromato-mass spectrometry and IR and PMR spectroscopy were used to study the high-temperature reaction of 2-bromocaproic, 2-iodocaproic, and 2-bromo-2-phenylacetic acids with acetonitrile.The formation of anomalous transnitrilation products (capronitrile and benzyl cyanide) is a consequence of the initial conversion of 2-halo-substituted caproic and phenylacetic acids to caproic and phenylacetic acids, respectively.
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