Tetrahedron Letters p. 5569 - 5572 (1996)
Update date:2022-08-24
Topics:
Kobayashi, Shu
Hachiya, Iwao
Yasuda, Masaru
Aldol reactions on solid phase have been achieved. In the presence of a catalytic amount of scandium triflate (Sc(OTf)3), polymer-supported silyl enol ethers reacted with aldehydes to afford the corresponding β-hydroxy thioester derivatives, which were reduced to 1,3-diol and β-hydroxy aldehyde derivatives, or hydrolyzed to β-hydroxy carboxylic acid derivatives.
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