Synthesis p. 28 - 30 (1995)
Update date:2022-08-11
Topics:
Yeager
Schissel
A convenient three-step method for the preparation of 2-aryloxyphenols from phenols and 2-fluorobenzaldehyde is described. Condensation of phenols with 2-fluorobenzaldehyde produces the intermediate 2-aryloxybenzaldehydes in 83-95% yield. These products rapidly undergo meta-chloroperbenzoic acid (m-CPBA) promoted Baeyer-Villiger oxidation to yield the corresponding 2-aryloxyphenyl formates which are hydrolyzed, without isolation, to give the desired 2-aryloxyphenols in 79-96% yield.
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Doi:10.1021/acs.joc.0c02424
(2021)Doi:10.1039/c8nj00368h
(2018)Doi:10.1016/j.ejmech.2020.112550
(2021)Doi:10.1246/bcsj.20150331
(2016)Doi:10.1002/anie.200801132
(2008)Doi:10.1016/S0040-4039(00)88041-7
(1983)
