Molecules p. 9986 - 9998 (2014)
Update date:2022-08-29
Topics:
Christiaens, Sylvain
Vantyghem, Xavier
Radoiu, Marilena
Eynde, Jean Jacques Vanden
Dialkyl 1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylates have been prepared in a batch mode under conventional heating as well as under continuous flow conditions in the Miniflow 200SS, Sairem's microwave- Assisted batch and continuous flow equipment. Real- Time monitoring of the reactions by Raman spectroscopy enabled to compare both heating modes and to determine (optimized) reaction times.
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