Tetrahedron Letters p. 1999 - 2000 (1985)
Update date:2022-08-10
Topics:
Felkin, Hugh
Fillebeen-Khan, Tauqir
Holmes-Smith, Rupert
Yingrui, Lin
The selective, catalytic conversion of methylcyclohexane into methylenecyclohexane at 100 deg C, and of n-hexane into 1-hexene at 45 deg C, has been effected using bis(triisopropylphosphine)iridium pentahydride and an olefin (neohexene) as a hydrogen acceptor; with this system, approximate relative reactivities of C-H bonds in saturated hydrocarbons are: sec-alkyl-H, 1; iso-alkyl-H, 8; n-alkyl-H, >60.
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