Journal of Molecular Structure p. 346 - 350 (2017)
Update date:2022-08-30
Topics:
Fatima, Tabinda
Haque, Rosenani A.
Razali, Mohd. R.
The tridentate N-heterocyclic carbenes (NHC) ligands derived from tris azolium salts by a new synthetic approach are described. The tris azolium salts have been obtained by reacting the initially synthesized precursor 3-(2-bromoethyl)-1-methylbenzimidazolium bromide (I) with benzimidazole/imidazole resulting in the tris azolium salts namely, 1 and 2. The ligand potential of the salts 1 and 2 was investigated by the formation of NHC-Ag(I) complexes 3 and 4, using Ag2O. The most downfield resonances in 13C NMR around 180–190?ppm indicates the successful coordination of carbene with Ag(I).
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