Journal of Organic Chemistry p. 4280 - 4283 (1980)
Update date:2022-08-29
Topics:
Gebeyehu, Gulilat
McNelis, Edward
The oxidation of diphenylacetylene with H5IO6 in acetic acid affords benzil.In methanol the principal products are the monoketal and the diketal of benzil, depending upon water content.Similar products are formed in methanol when I2O5 is the oxidizing agent.The latter and the alkyne in ethylene glycol afford benzil and the corresponding diketal.Both systems appear to require the presence of iodine for effective action.
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