Organic Letters p. 18 - 21 (2013)
Update date:2022-08-16
Topics:
Ye, Hui
Liu, Ruihua
Li, Dongmei
Liu, Yonghui
Yuan, Haixin
Guo, Weikang
Zhou, Lifei
Cao, Xuefeng
Tian, Hongqi
Shen, Jie
Wang, Peng George
A facile approach to the diazotransfer reagent of imidazole-1-sulfonyl azide was reported. The procedure was well optimized to clarify potential explosion risks. A high production yield as well as small batch variation was achieved even without careful pretreatment of reagents and solvents. HPLC and NMR methods to monitor the process were provided. These features made this protocol suitable for large scale preparation in academia and industry as well.
View MoreContact:0086-29-89196322
Address:North of the Fifth Keji Road, Hi-Tech Industrial Zone, Xi'an City, Shaanxi Province, China
Suzhou Jingye Medicine & Chemical Co., Ltd
website:http://www.jingyechem.cn
Contact:+86-512-66658588
Address:No. 88, Sanlian Street, Jinfeng Road, Suzhou New District, Jiangsu Province, P. R. China
Chemvon Biotechnology Co. Ltd.
website:http://www.chemvon.com
Contact:86-21-58550039;86-21-31268550-8004
Address:Suite B-10#, 6999 Chuansha Road, Pudong District, Shanghai 201202, China
Zhongshan Haihong Medicine Co., Ltd.
Contact:86-0760-86925778 (0)18824993998
Address:A7 building,lianyuan road Torch Hi-tech Industrial Development Zone
Shanghai KFSL Pharmaceutical Technology Co.,Ltd.
Contact:+86-21-39971718
Address:859 jiadingchengliu shanghai
Doi:10.1016/S0040-4039(99)00098-2
(1999)Doi:10.1021/jacs.1c03162
(2021)Doi:10.1002/adsc.201500941
(2016)Doi:10.1021/jacs.8b04699
(2018)Doi:10.1021/ja02248a009
(1917)Doi:10.1016/j.cclet.2021.05.016
(2021)