Tetrahedron Letters p. 4387 - 4390 (1998)
Update date:2022-08-28
Topics:
Millan, David S.
Prager, Rolf H.
Phenyl chlorothionoformate reacts reacts rapidly with aliphatic amines at 20°C to give a thiourethane and an alkyl chloride. The urethanes are readily converted to the secondary amine salt by reaction with dimethyl sulfate, followed by hydrolysis with wat
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