Journal of Chemical Crystallography p. 255 - 258 (2000)
Update date:2022-08-11
Topics:
Rangappa
Mallesha
Anilkumar
Yathirajan
Sridhar
Lokanath
Prasad, J. Shashidhara
The structures of the title compounds, tris(2-hydroxy-3-t-butyl-5-methylbenzene)-methane (C34H46O3.3H2O, 3) and N-benzyl-N-phenylbenzamide (C20H17NO, 6), have been investigated by X-ray crystallography. Compound 3 crystallizes in the trigonal space group P3 with cell parameters a = 14.090(5) A, b = 14.090(5)A, c = 10.485(5)A, Z= 2. Compound 6 crystallizes in the monoclinic space group C2/c with cell parameters a = 24.533(4)A, b =9.176(4)A, c = 16.711(5)A, β= 125.88(2)°, Z= 8. Compound 3 has both intra-and intermolecular hydrogen bonds. It also exhibits a helical columnar arrangement of the molecules and goes into mesophase before melting into an isotropic liquid.
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Doi:10.1039/b612770c
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