Journal of Organic Chemistry p. 11072 - 11079 (2020)
Update date:2022-08-25
Topics:
Llopis, Natalia
Gisbert, Patricia
Baeza, Alejandro
The straightforward synthesis of N,N-disubstituted formamides using a combination of 1,1,1,3,3,3-hexafluoroispropanol (HFIP) and H2O2 is described. The unique features of HFIP allowed the utilization of a green oxidant such as H2O2, and the products, arising from an oxidation-rearrangement sequence, were obtained in good to high yields under smooth reaction conditions.
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