Tetrahedron Letters p. 9157 - 9160 (1996)
Update date:2022-09-26
Topics:
Hollinshead, Sean P.
Resin bound 3-hydroxyacetophenone 2 was condensed (NaOMe/MeOH/THF) with aryl aldehydes to afford α,β-unsaturated ketones 3a-e. Subsequent reaction with azomethine ylid 5 in the presence of LiBr/DBU provided pyrrolidines 6a-d. These were subsequently acylated and cleaved from the solid support to afford highly functionalised pyrrolidines 8a-d.
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(1997)Doi:10.1007/BF00909814
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(1939)Doi:10.1021/jo01256a006
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(1999)
