Journal of Fluorine Chemistry p. 239 - 254 (1986)
Update date:2022-08-22
Topics:
Argentini, M.
Weinreich, R.
Oberti, Roberta
Ungaretti, Luciano
3-Deoxy-3-fluoro-1.2:5,6-di-O-isopropylidene-α-D-glucofuranose 4 has been synthesized and obtained crystalline.X-Ray structure analysis of the crystals has been performed.The space group was determined to be C2, a = 20.883 (12), b = 5.599 (1), c = 24.866 (13) Angstroem, β = 111.03 (3) deg.Two independent molecules are present in the asymmetric unit: on the basis of puckering parameters they show different conformations, which can be ascribed to crystal-packing requirements.
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