Journal of Organic Chemistry p. 2413 - 2417 (2015)
Update date:2022-08-17
Topics:
Chen, Wenwen
Zhang, Jianlan
Wang, Bo
Zhao, Zhouxing
Wang, Xinyan
Hu, Yuefei
A tandem synthesis for structurally novel 3-chloro-4-iodoisoxazoles was developed by simply mixing 1-copper(I) alkynes, dichloroformaldoxime, and molecular iodine together. The combination of 1-copper(I) alkyne and molecular iodine was well used as a synthetic equivalent of 1-iodoalkyne without the need for tedious preparation, purification, and storage of 1-iodoalkyne.
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