Archiv der Pharmazie p. 737 - 738 (1995)
Update date:2022-08-16
Topics:
Hauer
Ritter
Grotemeier
Isovanillin was oxidized with magnesium monoperoxyphthalate to 4-methoxyresorcinol (2) and the latter was reacted with 3-oxo-propionic acid ethylester prepared in situ to give scopoletin (1). These reactions can be achieved in kg scale in high yields.
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Doi:10.1021/jo01285a070
(1967)Doi:10.1016/S0040-4039(98)02570-2
(1999)Doi:10.1021/ja104158h
(2010)Doi:10.1039/c3cc47121g
(2013)Doi:10.1002/mrc.1260270803
(1989)Doi:10.1016/j.jallcom.2012.09.100
(2013)
