Bulletin of the Chemical Society of Japan p. 2432 - 2435 (1993)
Update date:2022-08-10
Topics:
Iwata, Satoru
Ishiguro, Yoshiharu
Utsugi, Masatuka
Mitsuhashi, Keiryo
Tanaka, Kiyoshi
Additions of various carbanion nucleophiles to 3,3,3-trifluoro-1-nitropropene (1) proceeded regiospecifically at the C-2 position of 1 to give the corresponding adducts.The nitro group of the adducts, derived from the reactions with acetylacetone and ethyl acetoacetate, was reduced to the corresponding amines, which were cyclized in situ to the 3-(trifluoromethyl)pyrrole derivatives.
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