Preparation of Trifluoromethylated Compounds by Anodic Oxidation of 3-Hydroxy-2-trifluoromethylpropionic Acid

DOI: 10.1246/cl.1987.1435

Source and publish data:

Chemistry Letters p. 1435 - 1438 (1987)

Update date:2022-08-16

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Authors:

Kubota, Toshio

Aoyagi, Ryouji

Sando, Hidehiro

Kawasumi, Masashi

Tanaka, Tatsuo

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Article abstract of DOI:10.1246/cl.1987.1435

Electrochemical Oxidation of 3-hydroxy-2-trifluoromethylpropionic acid (1) produced 2,3-bis(trifluoromethyl)-1,4-butanediol in quantitative yield.Furthermore, 2-trifluromethylated alcohols were obtained by the crossed Kolbe reaction of 1 with carboxylic acids or dicarboxylic acid mono esters.

Full text of DOI:10.1246/cl.1987.1435

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