Tetrahedron Letters p. 9083 - 9086 (2004)
Update date:2022-08-17
Topics:
Uno, Hidemitsu
Moriyama, Kana
Ishikawa, Takayuki
Ono, Noboru
Yahiro, Hidenori
The precursor was converted to thioindigo with P21/c structure by heating. 2,2′-Bi[-3(2H)-thiophenon]ylidene with two bicyclo[2.2.2]-octadiene moieties was quantitatively converted to thioindigo by the retro-Diels-Alder reaction. The thioindigo solid obtained from the precursor had the P21/c structure which was different from the commercial thioindigo samples (P21/n).
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