Tetrahedron Letters p. 961 - 964 (1998)
Update date:2022-08-17
Topics:
Benesch, Lisbeth
Bury, Paul
Guillaneux, Denis
Houldsworth, Stephen
Wang
Snieckus, Victor
2-Imino-2'-methyl biaryls, conveniently available by Suzuki cross coupling protocol, undergo lithium diethyl amide-mediated metalation - cyclization to give 9-aminophonanthrenes (Table 1). The application of this new general methodology to the first synthesis of the alkaloid piperolactam C (9) is described.
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