Bulletin of the Chemical Society of Japan p. 3349 - 3352 (1983)
Update date:2022-08-11
Topics:
Suginome
Maeda
Kaji
Takakuwa
Photolysis of 6-methylcholest-5-en-3 beta -ol nitrite and 4,4,6-trimethylcholest-5-en-3 beta -ol nitrite in benzene with monochromatic light respectively gave a seven-membered cyclic hydroxamic acid arising from rearrangement albeit in low yields. Photolysis of 3 alpha -methylcholest-5-en-3 beta -ol nitrite and 3 alpha ,4,4-trimethylcholest-5-en-3 beta -ol nitrite respectively gave a nitroso dimer arising from beta -scission.
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