Chemistry of Heterocyclic Compounds p. 1289 - 1292 (1992)
Update date:2022-08-17
Topics:
Koikov, L. N.
Lisitsa, E. A.
Alekseeva, N. A.
Turchin, K. F.
Filipenko, T. Ya.
3-Ethoxycarbonylquinuclidine obtained by the Grob method is a mixture of 3-ethoxycarbonyl-1-azabicyclo<2.2.2>- and, according to 13C NMR data, 5-ethoxycarbonyl-5-azatricyclo<3.2.1.02,7>octanes (about 16:2:1). 3-Ethoxy-carbonylquinuclidine was purified by recrystallization of the hydrochloride, hydrolyzed by water to 3-quinuclidinecarboxylic acid, and reduced by LiAlH4 to 3-quinuclidinylmethanol.
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