Chemistry of Natural Compounds p. 638 - 639 (1988)
Update date:2022-08-10
Topics:
Sorokin, V. L.
Kulinkovich, O. G.
4-Methylpent-3-enal has been synthesized by the dehydration of trans-2-(1-hydroxy-1-methylethyl)-1-methoxycyclopropane, and this has been brought into reaction with propen-2-ylmagnesium bromide.Acetylation of the carbinol so formed gave the acetate of (+/-)-2,6-dimethylhepta-1,5-diene-3-ol - the racemic form of the sex pheromone of the Comstock mealybug.
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