Journal of Organic Chemistry p. 5045 - 5047 (1993)
Update date:2022-08-12
Topics:
Ikenaga, Kazutoshi
Hiramatsu, Kouji
Nasaka, Norimitsu
Matsumoto, Satoshi
In the presence of triphenylphosphinepalladium complexes, (trialkylstannyl)dimethylsilane rapidly reacted at room temperature with terminal acetylenes to give 3,4-disubstituted 1-silacyclopenta-2,4-dienes in moderate yield.The formation of 1-silacyclopentadiene derivatives is evidence for the generation of dimethylsilylene species from (trialkylstannyl)dimethylsilane.
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