Bulletin of the Chemical Society of Japan p. 2183 - 2184 (1983)
Update date:2022-08-10
Topics:
Torii
Inokuchi
Kondo
Lepiochlorin is an antibiotic butenolide, a chlorinated metabolite of a fungus cultivated by a leaf-cutting ant. It was synthesized from 2-methyl-4-oxopentanoic acid by the electrochemical chloromethoxylation of 2-methyl-2,4-pentadien-4-olide in the MeOH-NH//4Cl-(Pt-Pt) system followed by hydrolysis in a mixed solution of dioxane-H//2O-concd HCl (25/10/1 V/V/V) in 38% overall yield. 14 reefs.
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(1959)
