Inorganica Chimica Acta p. 36 - 40 (2015)
Update date:2022-08-11
Topics:
Chan, Natalie H.
Roache, James H.
Jones, William D.
Cp?Co(C2H4)2 was reacted with benzothiophene and C-S activation of the vinyl-sulfur bond was observed. The resulting product, [Cp?Co]2(μ-κ2-C,S-C8H6S) was characterized by 1H NMR, 13C{1H} NMR, 13C DEPT-135 NMR, and 1H-13C 2D HSQC spectroscopies. The broad Cp? methyl peaks in these spectra suggested a fluxional structure.
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Doi:10.1002/chem.201902811
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