Tetrahedron Letters p. 7043 - 7044 (1993)
Update date:2022-08-11
Topics:
Staszak, Michael A.
Doecke, Christopher W.
N,O-bis(tert-butoxycarbonyl)hydroxylamine was synthesized in 85percent yield from hydroxylamine hydrochloride and di-tert-butyl dicarbonate in the presence of triethylamine.The chemistry is facile, utilizes readily available reagents and represents an improvement in safety over the previously published method.
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