A Facile Synthesis of N,O-bis(tert-butoxycarbonyl)-Hydroxylamine

Article abstract of DOI:10.1016/S0040-4039(00)61592-7

N,O-bis(tert-butoxycarbonyl)hydroxylamine was synthesized in 85percent yield from hydroxylamine hydrochloride and di-tert-butyl dicarbonate in the presence of triethylamine.The chemistry is facile, utilizes readily available reagents and represents an improvement in safety over the previously published method.