Carbohydrate Research p. 347 - 351 (1997)
Update date:2022-08-23
Topics:
Goggin, Kathleen D.
Lambert, Jack F.
Walinsky, Stanley W.
Thermal reaction of β-cellobiosyl fluoride heptaacetate with ticogenin in toluene or o-xylene at 112-142°C gave ticogenyl β-cellobioside heptaacetate in 69-75% yields with good stereoselectivity. The procedure avoids the use of Lewis acid or traditional glycosidation promoters. The deacetylated product is a hypocholesterolemic and anti-atherosclerosis agent.
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