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Cas Database

Name

N-methylhomoveratrylamine

EINECS

222-483-9

CAS No.

3490-06-0

Density

1.059

PSA

30.49000

LogP

1.85660

Solubility

N/A

Melting Point

N/A

Formula

C11H17 N O2

Boiling Point

294.4°Cat760mmHg

Molecular Weight

195.261

Flash Point

>110 ºC

Transport Information

N/A

Appearance

N/A

Safety

Hazard Codes	Xi
Risk Statements	36/37/38
Safety Statements	26-37/39
RIDADR	1760
WGK Germany	3
HazardClass	8
PackingGroup	III

Risk Codes

R36/37/38

Molecular Structure

Hazard Symbols

Synonyms

Phenethylamine,3,4-dimethoxy-N-methyl- (6CI,7CI,8CI);2-(3,4-Dimethoxyphenyl)-N-methylethanamine; 2-(3,4-Dimethoxyphenyl)-N-methylethylamine;3,4-Dimethoxy-N-methylbenzeneethanamine; 3,4-Dimethoxy-N-methylphenethylamine;3,4-Dimethoxy-N-methylphenylethylamine; 3,4-Dimethoxy-b-phenethylmethylamine;Methyl[2-(3,4-dimethoxyphenyl)ethyl]amine; N-(3,4-Dimethoxyphenethyl)-N-methylamine;N-Methyl-2-(3,4-dimethoxyphenyl)ethylamine; N-Methyl-3,4-dimethoxy-b-phenethylamine;N-Methyl-3,4-dimethoxy-b-phenylethylamine; N-Methyl-3,4-dimethoxybenzeneethanamine;N-Methyl-3,4-dimethoxyphenethylamine; N-Methylhomoveratrylamine; N-[2-(3,4-Dimethoxyphenyl)ethyl]-N-methylamine;NSC 187772; [2-(3,4-Dimethoxyphenyl)ethyl]methylamine

Article Data

N-methylhomoveratrylamine Synthetic route

: 40511-15-7
1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride

A: 3490-06-0
N-methylhomoveratrylamine

B: 5653-66-7
1-(3,4-dimethoxyphenyl)-2-(methylamino)ethan-1-ol

Conditions

Conditions	Yield
Stage #1: 1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride With hydrogen; 5%-palladium/activated carbon In water at 75℃; under 2585.81 Torr; for 16 - 40h; Stage #2: With sodium hydroxide In water; toluene pH=12; Product distribution / selectivity;	A n/a B 95.1%

: 14301-36-1
N-[2-(3,4-dimethoxyphenyl)ethyl]formamide

: 3490-06-0
N-methylhomoveratrylamine

Conditions

Conditions	Yield
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran 1) room temperature, 1 h; 2) reflux, 3 h;	90%
With tetrahydrofuran; lithium aluminium tetrahydride
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether

: 75803-23-5
methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester

: 74-89-5
methylamine

: 3490-06-0
N-methylhomoveratrylamine

Conditions

Conditions	Yield
Stage #1: methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester; methylamine In methanol; water at 140℃; under 15514.9 Torr; for 0.166667h; Flow reactor; Stage #2: With potassium hydroxide In water	90%

: 13230-71-2
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide

: 74-88-4
methyl iodide

: 3490-06-0
N-methylhomoveratrylamine

Conditions

Conditions	Yield
With sodium hydride In tetrahydrofuran for 4h; Ambient temperature;	82%

: 6380-23-0
3,4-dimethoxystyrene

: 3400-11-1
N-methylhydroxylamine-O-sulphonic acid

: 3490-06-0
N-methylhomoveratrylamine

Conditions

Conditions	Yield
Stage #1: 3,4-dimethoxystyrene With Schwartz's reagent In tetrahydrofuran at 25℃; Stage #2: N-methylhydroxylamine-O-sulphonic acid In tetrahydrofuran at 50℃; for 0.5h;	71%

: 27160-08-3
2-(3,4-dimethoxyphenyl)-ethylchloride

: 74-89-5
methylamine

: 3490-06-0
N-methylhomoveratrylamine

Conditions

Conditions	Yield
Stage #1: 2-(3,4-dimethoxyphenyl)-ethylchloride; methylamine In ethanol at 20℃; for 1h; Stage #2: With triisobutylaluminum In ethanol at 60℃; for 32h;	68%