4-Acetamidobenzene-d4-sulfonylChloride

Base Information Edit

Chemical Name:4-Acetamidobenzene-d4-sulfonylChloride
CAS No.:77435-44-0
Molecular Formula:C₈H₈ClNO₃S
Molecular Weight:237.644
Hs Code.:
DSSTox Substance ID:DTXSID701207876
Mol file:77435-44-0.mol

Synonyms:77435-44-0;4-Acetamidobenzene-d4-sulfonylChloride;4-Acetamidobenzene-1-sulfonyl chloride D4;4-ACETAMIDOBENZENE-D4-SULFONYL CHLORIDE;DTXSID701207876;HY-W012207S;CS-0129261;4-Acetamido-2,3,5,6-tetradeuteriobenzenesulfonyl chloride;Benzene-2,3,5,6-d4-sulfonyl chloride, 4-(acetylamino)-

Suppliers and Price of 4-Acetamidobenzene-d4-sulfonylChloride

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 4 raw suppliers

Chemical Property of 4-Acetamidobenzene-d4-sulfonylChloride Edit

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:237.0164490
Heavy Atom Count:14
Complexity:301

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)NC1=CC=C(C=C1)S(=O)(=O)Cl
Isomeric SMILES:[2H]C1=C(C(=C(C(=C1NC(=O)C)[2H])[2H])S(=O)(=O)Cl)[2H]

Technology Process of 4-Acetamidobenzene-d4-sulfonylChloride

There total 4 articles about 4-Acetamidobenzene-d4-sulfonylChloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 15826-91-2
acetanilide-d5

: 77435-44-0
p-acetamidobenzenesulfonyl chloride-d₄

Guidance literature:: With chlorosulfonic acid; at 25 - 30 ℃; for 3h; Time;

Reference yield:

: 4165-60-0
nitrobenzene-d5

: 77435-44-0
p-acetamidobenzenesulfonyl chloride-d₄

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; ammonium formate / methanol / 0.33 h / Inert atmosphere; Reflux

2: 20 °C / Inert atmosphere; Cooling with ice

3: chlorosulfonic acid / 20 °C / Inert atmosphere; Cooling with ice

With chlorosulfonic acid; palladium 10% on activated carbon; ammonium formate; In methanol;
DOI:10.1002/jlcr.1741

Reference yield:

: 4165-61-1
aniline-d5

: 77435-44-0
p-acetamidobenzenesulfonyl chloride-d₄

Guidance literature:: Multi-step reaction with 2 steps

1: 20 °C / Inert atmosphere; Cooling with ice

2: chlorosulfonic acid / 20 °C / Inert atmosphere; Cooling with ice

With chlorosulfonic acid;
DOI:10.1002/jlcr.1741

upstream raw materials:

Downstream raw materials:

p-[⁽²⁾H₄]-nitrobenzenesulfonic acid

p-[⁽²⁾H₄]-nitrobenzenesulfonyl chloride

p-[⁽²⁾H₄]-aminobenzene sulfonic acid

sulfamethazine-d4

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Encyclopedia

Technology Process of 4-Acetamidobenzene-d4-sulfonylChloride

4-Acetamidobenzene-d4-sulfonylChloride

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