4-Methylenecyclohexanone

Base Information

Chemical Name:4-Methylenecyclohexanone
CAS No.:29648-66-6
Molecular Formula:C7H10O
Molecular Weight:110.156
Hs Code.:
Mol file:29648-66-6.mol

Synonyms:monoethylene ketal;Cyclohexanone,4-methylene;1,4 cyclohexanedione;Cyclohexanone,4-methylidene;4-Methylenecyclohexanone;

Suppliers and Price of 4-Methylenecyclohexanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
4-Methylenecyclohexanone 97%
10g
$ 2700.00

Matrix Scientific
4-Methylenecyclohexanone 97%
5g
$ 1764.00

Total 8 raw suppliers

Chemical Property of 4-Methylenecyclohexanone

Chemical Property:

PSA：17.07000
LogP:1.68570

Purity/Quality:

97% ^*data from raw suppliers

4-Methylenecyclohexanone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Methylenecyclohexanone

There total 6 articles about 4-Methylenecyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 51656-90-7
8-methylene-1,4-dioxaspiro[4.5]decane

: 29648-66-6
4-methylenecyclohexanone

Guidance literature:: With water; pyridinium p-toluenesulfonate; In acetone; for 6h; Heating;
DOI:10.1016/S0040-4020(98)00788-1

Reference yield:

: 4746-97-8
cyclohexanedione monoethylene ketal

: 29648-66-6
4-methylenecyclohexanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: BuLi / tetrahydrofuran; pentane / 1 h / 20 °C

1.2: 69 percent / tetrahydrofuran; pentane / 15 h / 20 °C

2.1: 90 percent / H₂SO₄; silica gel / CH₂Cl₂ / 6 h

With n-butyllithium; sulfuric acid; silica gel; In tetrahydrofuran; dichloromethane; pentane;
DOI:10.1135/cccc20021517