4-[(METHOXYCARBONYL)AMINO]BENZOIC ACID

Base Information

• Chemical Name: 4-[(METHOXYCARBONYL)AMINO]BENZOIC ACID
• CAS No.: 30063-17-3
• Molecular Formula: C9H9NO4
• Molecular Weight: 195.175
• Mol file: 30063-17-3.mol

Synonyms:4-Methoxycarbonylamino-benzoesaeure;(4-Carboxy-phenyl)-carbamidsaeure-methylester;4-(methoxycarbonylamino)benzoic acid;

Chemical Property of 4-[(METHOXYCARBONYL)AMINO]BENZOIC ACID

Chemical Property:

• PSA: 75.63000
• LogP: 1.63610

Purity/Quality:

99% ^*data from raw suppliers

4-(Methoxycarbonylamino)benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[(METHOXYCARBONYL)AMINO]BENZOIC ACID

There total 6 articles about 4-[(METHOXYCARBONYL)AMINO]BENZOIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

4-amino-benzoic acid (150-13-0,159246-81-8,8014-65-1) + methyl chloroformate (79-22-1) → 4-[(methoxycarbonyl)amino]benzoic acid (30063-17-3)

Guidance literature:

With sodium sulfate; In 1,4-dioxane; at 70 ℃; for 2.25h;

DOI:10.1002/1099-0690(200011)2000:22<3755::aid-ejoc3755>3.0.co;2-i

Reference yield: 70.0%

methanol (67-56-1) + potassium cyanate (590-28-3) + 4-Bromobenzoic acid (586-76-5) → 4-[(methoxycarbonyl)amino]benzoic acid (30063-17-3)

Guidance literature:

With copper(l) iodide; 2-(2,6-dimethylphenyl-amino)-2-oxoacetic acid potassium salt; at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1002/adsc.201200296

Reference yield: 54.0%

methyl 4-((methoxycarbonyl)amino)benzoate (94563-12-9) → 4-[(methoxycarbonyl)amino]benzoic acid (30063-17-3)

Guidance literature:

With sodium hydroxide; at 60 - 70 ℃; for 8h;

DOI:10.1021/jm970479e

upstream raw materials:

4-amino-benzoic acid

methyl chloroformate

methanol

carbon monoxide

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