3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-

Base Information

Chemical Name:3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-
CAS No.:30182-86-6
Molecular Formula:C18H16N2O2
Molecular Weight:292.337
Hs Code.:
DSSTox Substance ID:DTXSID10405466
Nikkaji Number:J1.078.502B
Wikidata:Q82210036

Synonyms:30182-86-6;4-Benzoyl-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one;3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-;DTXSID10405466

Suppliers and Price of 3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:292.121177757
Heavy Atom Count:22
Complexity:485

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=O)N(N1C)C2=CC=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of 3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-

There total 18 articles about 3H-Pyrazol-3-one, 4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 60-80-0
antipyrine

: 611-73-4
Benzoylformic acid

: 30182-86-6
4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-3H-pyrazol-3-one

Guidance literature:: With dipotassium peroxodisulfate; copper diacetate; In methanol; water; at 60 ℃; for 4h; Reagent/catalyst; Solvent; Catalytic behavior; Mechanism; Green chemistry;
DOI:10.1002/adsc.201800464

Reference yield: 83.0%

: 60-80-0
antipyrine

: 100-52-7
benzaldehyde

: 30182-86-6
4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-3H-pyrazol-3-one

Guidance literature:: With dipotassium peroxodisulfate; copper diacetate; In methanol; water; at 80 ℃; for 12h; Reagent/catalyst; Solvent; Temperature; Catalytic behavior; Mechanism; Schlenk technique; Sealed tube;
DOI:10.1039/c9ob01486a

Reference yield: 73.0%

: 129-81-7
iodoantipyrine

: 98-88-4
benzoyl chloride

: 30182-86-6
4-benzoyl-1,2-dihydro-1,5-dimethyl-2-phenyl-3H-pyrazol-3-one

Guidance literature:: iodoantipyrine; With diisopropylmagnesium; In dichloromethane; at -25 ℃; for 2h;

In dichloromethane;

benzoyl chloride; In tetrahydrofuran;