μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate)

Base Information

Chemical Name:μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate)
CAS No.:1086594-99-1
Molecular Formula:C₇₄H₄₂Ge₂N₁₂O₉
Molecular Weight:1388.4
Hs Code.:

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Chemical Property of μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate)

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Technology Process of μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate)

There total 1 articles about μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 67-56-1
methanol

: 7631-99-4
sodium nitrate

: 1027776-92-6
methoxy germanium(IV) meso-triphenylcorrolate

: 108-24-7
acetic anhydride

: 64-19-7,77671-22-8
acetic acid

: 1086595-01-8
methoxy germanium(IV) 3,17-dinitro-triphenylcorrolate

: μ-oxo digermanium(IV) bis(3-nitro-triphenylcorrolate)

: 1086594-99-1
μ-oxo digermanium(IV) bis(3,17-dinitro-triphenylcorrolate)

Guidance literature:: In acetic anhydride; acetic acid; Ge compd. and NaNO3 dissolved in (CH3CO)2O; stirred at 45°C; acetic acid added; stirred for 30 min; solvent evapd.; dissolved in CH2Cl2; washed (satd. aq. NaHCO3); org. phase concd.; sepd. by chromy. (neutral alumina, CH2Cl2); crystd. from CH2Cl2-hexane (μ-oxo dimer); eluted with CHCl3, crystd. from CH2Cl2-MeOH (Ge-OMe compd.); elem. anal.;
DOI:10.1021/ic801421a