mer-(CO)3(P(OPh)3)2WNCEt

Base Information

• Chemical Name: mer-(CO)3(P(OPh)3)2WNCEt
• CAS No.: 136086-69-6
• Molecular Formula: C₄₂H₃₅NO₉P₂W
• Molecular Weight: 943.539
• Mol file: 136086-69-6.mol

Synonyms:

Chemical Property of mer-(CO)3(P(OPh)3)2WNCEt

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of mer-(CO)3(P(OPh)3)2WNCEt

There total 3 articles about mer-(CO)3(P(OPh)3)2WNCEt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Dichloromethylsilane (75-54-7) + fac-(CO)3(P(OPh)3)2WNCEt (136086-69-6) → (CO)3(P(OC6H5)3)2W(H)(SiCl2CH3) + mer-(CO)3(P(OPh)3)2WNCEt (136086-69-6)

Guidance literature:

In dichloromethane; N2;; concd.; washed with CH2Cl2 and hexane; elem. anal.;;

DOI:10.1016/0022-328X(91)83037-5

Reference yield:

fac-(CO)3(P(OPh)3)2WNCEt (136086-69-6) + diphenylsilyl chloride (1631-83-0) → (CO)3(P(OC6H5)3)2W(H)(SiCl(C6H5)2) + mer-(CO)3(P(OPh)3)2WNCEt (136086-69-6)

Guidance literature:

In dichloromethane; N2;; concd.; washed with CH2Cl2 and hexane; elem. anal.;;

DOI:10.1016/0022-328X(91)83037-5

Reference yield:

fac-(CO)3(P(OPh)3)2WNCEt (136086-69-6) + trichlorosilane (10025-78-2) → mer-(CO)3(P(OPh)3)2WNCEt (136086-69-6) + (CO)3(P(OC6H5)3)2W(H)(SiCl3)

Guidance literature:

In dichloromethane; N2;; concd.; washed with CH2Cl2 and hexane; elem. anal.;;

DOI:10.1016/0022-328X(91)83037-5

upstream raw materials:

Dichloromethylsilane

diphenylsilyl chloride

trichlorosilane