Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-

Base Information

Chemical Name:Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-
CAS No.:30853-94-2
Molecular Formula:C31H35NOP2
Molecular Weight:499.573
Hs Code.:
DSSTox Substance ID:DTXSID50462871
Nikkaji Number:J1.317.276E
Wikidata:Q82287489
Mol file:30853-94-2.mol

Synonyms:30853-94-2;2-(Diphenylphosphino)-N-(2-(diphenylphosphino)ethyl)-N-(2-methoxyethyl)ethanamine;2-(Diphenylphosphino)-N-[2-(diphenylphosphino)ethyl]-N-(2-methoxyethyl)ethanamine;Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-;SCHEMBL5039710;DTXSID50462871;bis(2-diphenylphosphino-ethyl)-2-methoxyethylamine

Suppliers and Price of Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-

Chemical Property:

XLogP3:5.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:13
Exact Mass:499.21938874
Heavy Atom Count:35
Complexity:456

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COCCN(CCP(C1=CC=CC=C1)C2=CC=CC=C2)CCP(C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy-

There total 1 articles about Ethanamine, N,N-bis[2-(diphenylphosphino)ethyl]-2-methoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27807-62-1
bis-(2-chloro-ethyl)-(2-methoxy-ethyl)-amine; hydrochloride

: 15475-27-1,4346-39-8
potassium diphenylphosphine

: 30853-94-2
N-(2-methoxyethyl)-2-(diphenylphosphino)-N-(2-(diphenylphosphino)ethyl)ethanamine

Guidance literature:: In 1,4-dioxane;
DOI:10.1039/j19710000492

Reference yield: 94.0%

: [Tc(N)Cl₂(P(C₆H₅)3)2]

: 30853-94-2
N-(2-methoxyethyl)-2-(diphenylphosphino)-N-(2-(diphenylphosphino)ethyl)ethanamine

: fac-[Tc(N)Cl₂(bis[(2-diphenylphosphino)ethyl]methoxy-ethylamine)]

Guidance literature:: In dichloromethane; refluxed for 40 min; slowly evapd., residue was vigorously stirred in Et2O, washed with Et2O;elem. anal.;
DOI:10.1021/ja0200239

Reference yield: 80.0%

: 113945-92-9
dichlorobis(triphenylphosphine)nitridotechnetium(V)

: 30853-94-2
N-(2-methoxyethyl)-2-(diphenylphosphino)-N-(2-(diphenylphosphino)ethyl)ethanamine

: 148-18-5
sodium N,N-diethyldithiocarbamate

: 784153-36-2
[(bis[(diphenylphosphanyl)ethyl]methoxyethylamine)(N,N-(diethyl)dithiocarbamate)nitrido⁽⁹⁹⁾technetium(V)]Cl

Guidance literature:: In ethanol; dichloromethane; under N2; soln. of phosphane in ethanol added to suspn. of Tc complex (1equiv.) in CH2Cl2, mixt. stirred at room temp. for 1 h, soln. of dithio carbamate (excess) in ethanol added, mixt. refluxed for 1 h; cooled, evapd. (N2 stream), CH2Cl2 added, filtered, filtrate evapd. to dryness, residue treated with ethanol, ppt. filtered off, washed with diethyl ether, dried under vac.; elem. anal.;
DOI:10.1002/ejic.200300666