N-(1,3,4,6,7,11bα-hexahydro-7α-phenyl-2H-benzoquinolizin-2α-yl)-N',N'-dimethyl-N-phenylurea

Base Information

• Chemical Name: N-(1,3,4,6,7,11bα-hexahydro-7α-phenyl-2H-benzo
• Molecular Formula: C₂₈H₃₁N₃O
• Molecular Weight: 425.574

Synonyms:

Chemical Property of N-(1,3,4,6,7,11bα-hexahydro-7α-phenyl-2H-benzo

Chemical Property:

Purity/Quality:

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Useful:

There total 1 articles about N-(1,3,4,6,7,11bα-hexahydro-7α-phenyl-2H-benzoquinolizin-2α-yl)-N',N'-dimethyl-N-phenylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + (2α,7α,11bα)-1,3,4,6,7,11b-hexahydro-N,7-diphenyl-2H-benzoquinolizin-2-amine (75715-72-9) + dimethyl amine (124-40-3) → N-(1,3,4,6,7,11bα-hexahydro-7α-phenyl-2H-benzoquinolizin-2α-yl)-N',N'-dimethyl-N-phenylurea (87680-29-3)

Guidance literature:

Yield given. Multistep reaction; 1) CH₂Cl₂, 23 deg C, 1 h, 2) CH₂Cl₂, 23 deg C, 16 h;

DOI:10.1021/jo00173a054

upstream raw materials:

phosgene

(2α,7α,11bα)-1,3,4,6,7,11b-hexahydro-N,7-diphenyl-2H-benzoquinolizin-2-amine

dimethyl amine

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