Trimethylsilyl fluorosul-fonate

Base Information

Chemical Name:Trimethylsilyl fluorosul-fonate
CAS No.:3167-56-4
Molecular Formula:C3H9FO3SSi
Molecular Weight:172.253
Hs Code.:
DSSTox Substance ID:DTXSID201269697
Nikkaji Number:J1.021.214F
Mol file:3167-56-4.mol

Synonyms:trimethylsilyl fluorosul-fonate;SCHEMBL1903798;DTXSID201269697;Fluorosulfuric acid, trimethylsilyl ester;3167-56-4

Suppliers and Price of Trimethylsilyl fluorosul-fonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Trimethylsilyl fluorosul-fonate

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:172.00257001
Heavy Atom Count:9
Complexity:174

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C[Si](C)(C)OS(=O)(=O)F

Technology Process of Trimethylsilyl fluorosul-fonate

There total 2 articles about Trimethylsilyl fluorosul-fonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1206-46-8
trimethyl(pentafluorophenyl)silane

: 363-72-4
Pentafluorobenzene

: 3167-56-4
trimethylsilyl fluorosulfonate

Guidance literature:: With fluorosulphonic acid; In neat (no solvent); at -20 ℃; for 0.116667h; Yield given;
DOI:10.1016/S0022-328X(98)00805-5

Reference yield:

: 503027-47-2,503027-48-3,155139-78-9,18156-25-7
N,N'-bis(trimethylsilyl)sulfurdiimide

: 7789-21-1
fluorosulphonic acid

: 13446-08-7
ammonium fluorosulfonate

: 3167-56-4
trimethylsilyl fluorosulfonate

Guidance literature:: In neat (no solvent); exclusion of moisture; condensation of F-compd. and Si-compd. in NMR-tube (-80°C), shaking, warming (-40°C), warming (2 h, -10°C), warming (5 h, 20°C); not isolated; (1)H-NMR-spctroscopy;