Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]-

Base Information

• Chemical Name: Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]-
• CAS No.: 19980-35-9
• Molecular Formula: C10H20OSi
• Molecular Weight: 184.354
• DSSTox Substance ID: DTXSID50404135
• Nikkaji Number: J271.100A
• Wikidata: Q82208145

Synonyms:Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]-;19980-35-9;trimethyl-(2-methylcyclohexen-1-yl)oxysilane;SCHEMBL818161;DTXSID50404135;AKOS024339588

Chemical Property of Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]-

Chemical Property:

• PSA: 9.23000
• LogP: 3.68590
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 184.128341792
• Heavy Atom Count: 12
• Complexity: 189

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=C(CCCC1)O[Si](C)(C)C

Technology Process of Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]-

There total 17 articles about Silane, trimethyl[(2-methyl-1-cyclohexen-1-yl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

chloro-trimethyl-silane (75-77-4) + 2-Methylcyclohexanone (583-60-8) → 1-trimethylsilyloxy-2-methyl-1-cyclohexene (19980-35-9) + 6-methyl-1-trimethylsiloxycyclohex-1-ene (19980-33-7)

Guidance literature:

With N,N,N,N,N,N-hexamethylphosphoric triamide; bromomagnesium diisopropylamide; triethylamine; In diethyl ether; at 25 ℃; for 8h; Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.1016/S0040-4039(00)81652-4

Reference yield: 90.0%

chloro-trimethyl-silane (75-77-4) + 2-Methylcyclohexanone (583-60-8) → 1-trimethylsilyloxy-2-methyl-1-cyclohexene (19980-35-9)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; for 13h; Heating;

Reference yield: 82.0%

2-Methylcyclohexanone (583-60-8) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → (2-Methyl-cyclohex-1-enyl)-[2-methyl-cyclohex-(E)-ylidene]-amine + 1-trimethylsilyloxy-2-methyl-1-cyclohexene (19980-35-9) + Trimethyl-(2-methyl-cyclohexyloxy)-silane (109283-59-2)

Guidance literature:

With 1,1,1,3,3,3-hexamethyl-disilazane; cobalt(II) bromide; In toluene; at 110 ℃; for 6h;

DOI:10.1080/00397910600946033

upstream raw materials:

chloro-trimethyl-silane

2-chloro-2-methylcyclohexanone

2-Methylcyclohexanone

3-(trimethylsilyl)-2-oxazolidinone

Downstream raw materials:

2-methyl-2-(2-oxopropyl)cyclohexanone

2-bromo-2-methylcyclohexanone

2-methyl-2-(2-oxobutyl)cyclohexanone

2-methyl-2-(1-methyl-2-oxopropyl)cyclohexanone

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