N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide

Base Information

Chemical Name:N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide
CAS No.:7508-72-7
Molecular Formula:C16H14N2O
Molecular Weight:250.3
Hs Code.:
NSC Number:404151
DSSTox Substance ID:DTXSID70425948

Synonyms:N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide;N'-[(1E,2E)-3-phenylprop-2-en-1-ylidene]benzohydrazide;7508-72-7;PhCON2 cinnamal;NSC404151;SCHEMBL711311;SCHEMBL711312;SCHEMBL9374574;DTXSID70425948;STK215200;AKOS001608031;NSC-404151;(E)-N'-[(E)-3-Phenylallylidene]benzohydrazide;SR-01000076644;N'-(3-PHENYL-2-PROPENYLIDENE)BENZOHYDRAZIDE;SR-01000076644-1

Suppliers and Price of N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide

Chemical Property:

XLogP3:3.3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:250.110613074
Heavy Atom Count:19
Complexity:324

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC=NNC(=O)C2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)/C=C/C=N/NC(=O)C2=CC=CC=C2

Technology Process of N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide

There total 2 articles about N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 613-94-5
benzoic acid hydrazide

: 104-55-2
3-phenyl-propenal

: 7508-72-7
1-benzoyl-2-cinnamylidenehydrazine

Guidance literature:: at 99 ℃; for 0.0416667h; microwave irradiation;

Reference yield:

: 65-85-0,8013-63-6
benzoic acid

: 7508-72-7
1-benzoyl-2-cinnamylidenehydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. hydrazine hydrate / 4 h / 90 °C

2: 93 percent / 0.04 h / 99 °C / microwave irradiation

With hydrazine hydrate;

Reference yield: 93.0%

: 108-89-4
picoline

: copper(II) chloride hydrate

: 7508-72-7
1-benzoyl-2-cinnamylidenehydrazine

: 950488-06-9
CuCl((C₆H₅)2(CH)3N₂CO)(C₅H₄NCH₃)

Guidance literature:: In ethanol; soln. of ligand in EtOH added to hot (50-55°C) EtOH soln. of CuCl2*nH2O and 4-picoline pH 8, heated for 30-40 min with stirring, cooled; filtered, washed with alcohol and ether, dried in air; elem. anal.;
DOI:10.1134/S1070363206100161