3-BROMO-5-IODOANILINE

Base Information

• Chemical Name: 3-BROMO-5-IODOANILINE
• CAS No.: 31948-87-5
• Molecular Formula: C6H5BrIN
• Molecular Weight: 297.921
• Hs Code.: 2921420090
• Mol file: 31948-87-5.mol

Synonyms:3-Brom-5-iodanilin;3-BROMO-5-IODO-PHENYLAMINE;

Chemical Property of 3-BROMO-5-IODOANILINE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 335.486oC at 760 mmHg
• PKA: 2.56±0.10(Predicted)
• Flash Point: 156.696oC
• PSA: 26.02000
• Density: 2.292g/cm3
• LogP: 3.21710

Purity/Quality:

97% ^*data from raw suppliers

3-Bromo-5-iodoaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BROMO-5-IODOANILINE

There total 5 articles about 3-BROMO-5-IODOANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-bromo-3-iodo-5-nitrobenzene (861601-15-2) → 3-Bromo-5-iodoaniline (31948-87-5)

Guidance literature:

With iron; acetic acid; at 20 ℃; for 16h;

Reference yield: 67.0%

(3-bromo-5-iodophenyl)carbamic acid tert-butyl ester (915413-42-2) → 3-Bromo-5-iodoaniline (31948-87-5)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 12h;

Reference yield:

3-bromo-5-iodo-benzoic acid (188815-32-9) → 3-Bromo-5-iodoaniline (31948-87-5)

Guidance literature:

Multi-step reaction with 3 steps

1: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / methanol / 12 h / 20 °C

2: toluene / 2 h / Reflux

3: hydrogenchloride / 1,4-dioxane; water / 12 h / 20 °C

With hydrogenchloride; diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; methanol; water; toluene; 2: Curtius rearrangement;

DOI:10.1021/jm100659v

upstream raw materials:

1-bromo-3-iodo-5-nitrobenzene

(3-bromo-5-iodophenyl)carbamic acid tert-butyl ester

3-bromo-5-iodobenzoylazide

3-bromo-5-iodo-benzoic acid

Downstream raw materials:

1-benzoyl-3-(3-bromo-5-iodophenyl)thiourea

(3-bromo-5-iodo-phenyl)-carbamic acid methyl ester

N-(3-bromo-5-(6-methoxypyridin-3-yl)phenyl)acetamide

N-(3-bromo-5-(pyridin-4-yl)phenyl)methanesulfonamide

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