8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile

Base Information

• Chemical Name: 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile
• CAS No.: 58373-67-4
• Molecular Formula: C₂₈H₃₂N₄O₂
• Molecular Weight: 456.588

Synonyms:

Chemical Property of 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile

There total 1 articles about 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Acetic acid (1R,4R,8S,11S)-1,12,12-tricyano-6,10-dimethyl-4-(2,6,6-trimethyl-cyclohex-1-enyl)-3-aza-tricyclo[6.3.1.02,7]dodeca-2,6,9-trien-11-ylmethyl ester (58373-67-4)

Guidance literature:

Vitamin A1-Acetat, 1) Tetracyanoethylen, 2) erhitzen;

DOI:10.1002/hlca.19750580321

Reference yield:

methanol (67-56-1) + 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile (58373-67-4) → (7aRS)-3-imino-5t-[(3Ξ,6SR)-2-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-3,6-dihydro-pyridin-3-yl]-7-methyl-(3aξ,7ar)-3,3a,5,7a-tetrahydro-1H-isobenzofuran-4,4-dicarbonitrile (56924-64-2)

Guidance literature:

With potassium methanolate;

DOI:10.1002/hlca.19750580322

Reference yield:

sodium methylate (124-41-4) + 8t-acetoxymethyl-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-2,3,5,8-tetrahydro-5r,9c-methano-cyclohepta[b]pyridine-9,10,10-tricarbonitrile (58373-67-4) → 9-imino-10-methoxy-4,6-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-(4br,9aξ)-3,4b,6a,7,9,9a-hexahydro-2H-furo[3',4':5,6]benzo[1,2-c][1,8]naphthyridine-9bc-carbonitrile (56874-89-6) + 11-cyano-10-imino-4,7-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-(7ac)-3,5,7a,8-tetrahydro-2H-5r,10ac-methano-furo[3',4':6,7]cyclohepta[1,2-b]pyridine-11ξ-carboximidic acid methyl ester

Guidance literature:

In methanol;

DOI:10.1002/hlca.19750580322

Downstream raw materials:

(7aRS)-3-imino-5t-[(3Ξ,6SR)-2-methoxy-4-methyl-6-(2,6,6-trimethyl-cyclohex-1-enyl)-3,6-dihydro-pyridin-3-yl]-7-methyl-(3aξ,7ar)-3,3a,5,7a-tetrahydro-1H-isobenzofuran-4,4-dicarbonitrile

9-imino-10-methoxy-4,6-dimethyl-2c-(2,6,6-trimethyl-cyclohex-1-enyl)-(4br,9aξ)-3,4b,6a,7,9,9a-hexahydro-2H-furo[3',4':5,6]benzo[1,2-c][1,8]naphthyridine-9bc-carbonitrile

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