Technology Process of Benzene, [(1-methylethyl)telluro]-
There total 8 articles about Benzene, [(1-methylethyl)telluro]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diphenyl ditelluride;
In
benzene;
byproducts: PhTeHgCl; Irradiation (UV/VIS); nitrogen atmosphere; mercurial and PhTeTePh in deoxygenated solvent irradiated (275-W sunlamp, 35-40 °C, 4h);; filtration; solvent removed (vacuum); (CH3)2CHTePh analysed by (1)H NMR, GLC and GCMS;;
DOI:10.1021/ja00219a030
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; samarium diiodide;
In
tetrahydrofuran;
for 3h;
Heating;
1.) THF, RT, 2.) THF, reflux, 3 h;
DOI:10.1080/00397919308009767
- Guidance literature:
-
phenyllithium;
With
tellurium;
In
tetrahydrofuran; diethyl ether; cyclohexane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
isopropyl bromide;
In
tetrahydrofuran; diethyl ether; cyclohexane;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1002/anie.201709946
