Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]-

Base Information

Chemical Name:Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]-
CAS No.:327096-47-9
Molecular Formula:C14H14BNO2
Molecular Weight:239.082
Hs Code.:

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Suppliers and Price of Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]-

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Technology Process of Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]-

There total 1 articles about Boronic acid, [2-[[(3-methylphenyl)imino]methyl]phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 40138-16-7
2-formylbenzene boronic acid

: 108-44-1
1-amino-3-methylbenzene

: 327096-47-9
N-(2-dihydroxyborylbenzylidene)-m-tolylamine

Guidance literature:: In ethanol; m-toluidine and 2-formylbenzeneboronic acid were mixed in abs. EtOH and heated at reflux with aseotropic removal of water for 18 h; react. mixt. was cooled, solvent was removed in vacuo;
DOI:10.1039/b108896c

Reference yield: 81.0%

: 16940-66-2
sodium tetrahydroborate

: 327096-47-9
N-(2-dihydroxyborylbenzylidene)-m-tolylamine

: 262352-25-0
N-(2-dihydroxyborylbenzyl)-m-tolylamine

Guidance literature:: In methanol; NaBH4 was added slowly to Schiff base in dry methanol and stirred at room temp. for 2 h; react. mixt. was poured into ice-water, HCl was added slowly and stirredfor 30 min, ppt. was filtered; elem. anal.;
DOI:10.1039/b108896c